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Palladium N-Heterocyclic Carbene Catalysts for the Ultrasound-Promoted Suzuki-Miyaura Reaction in Glycerol
dc.contributor.author | Azua Barrios, Arturo | |
dc.contributor.author | Mata Martínez, Jose A | |
dc.contributor.author | Heymes, Pauline | |
dc.contributor.author | Peris, Eduardo | |
dc.contributor.author | Lamaty, Frederic | |
dc.contributor.author | Martínez, Jean | |
dc.contributor.author | Colacino, Evelina | |
dc.date.accessioned | 2014-06-10T06:58:59Z | |
dc.date.available | 2014-06-10T06:58:59Z | |
dc.date.issued | 2013-04-15 | |
dc.identifier.citation | AZUA BARRIOS, A.; MATA MARTÍNEZ, J. A.; HEYMES, P.; PERIS FAJARNÉS, E.; LAMATY, F.; MARTÍNEZ, J.; COLACINO, E. Palladium N-Heterocyclic Carbene Catalysts for the Ultrasound-Promoted Suzuki-Miyaura Reaction in Glycerol. Advanced Synthesis & Catalysis, Volume 355, Issue 6 (April 15, 2013), p. 1107-1116 | ca_CA |
dc.identifier.uri | http://hdl.handle.net/10234/94532 | |
dc.description.abstract | Novel palladium N-heterocyclic-carbene (NHC)-based complexes with 3,4,5-trimethoxybenzyl, alkyl and sulfonate N-substituents were obtained and fully characterized. The new complexes were used as pre-catalysts in the Suzuki–Miyaura coupling of various aryl halides/boron sources in glycerol under pulsed-ultrasound (P-US) activation. High yields were obtained under mild reaction conditions, without formation of undesired by-products. The pure final cross-coupling products were easily recovered without column chromatography and the catalytic/solvent system could be recycled. TEM (transmission electron microscopy) and XPS (X-ray photoelectron spectroscopy) were used to characterize the nanoparticles and to investigate the fate of the catalysts. | ca_CA |
dc.format.extent | 10 p. | ca_CA |
dc.format.mimetype | application/pdf | ca_CA |
dc.language.iso | eng | ca_CA |
dc.publisher | Wiley | ca_CA |
dc.relation.isPartOf | Advanced Synthesis & Catalysis, Volume 355, Issue 6 (April 15, 2013) | ca_CA |
dc.rights.uri | http://rightsstatements.org/vocab/CNE/1.0/ | * |
dc.subject | Green chemistry | ca_CA |
dc.subject | Glycerol | ca_CA |
dc.subject | N-heterocyclic carbenes | ca_CA |
dc.subject | Sonication | ca_CA |
dc.subject | Suzuki–Miyaura reaction | ca_CA |
dc.subject | XPS | ca_CA |
dc.subject | X-ray photoelectron spectroscopy | ca_CA |
dc.title | Palladium N-Heterocyclic Carbene Catalysts for the Ultrasound-Promoted Suzuki-Miyaura Reaction in Glycerol | ca_CA |
dc.type | info:eu-repo/semantics/article | ca_CA |
dc.identifier.doi | http://dx.doi.org/10.1002/adsc.201201047 | |
dc.rights.accessRights | info:eu-repo/semantics/restrictedAccess | ca_CA |
dc.relation.publisherVersion | http://onlinelibrary.wiley.com/doi/10.1002/adsc.201201047/abstract | ca_CA |
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