Synthesis of wurtzite ZnS nanoparticles using the microwave assisted solvothermal method
Impacto
Scholar |
Otros documentos de la autoría: La Porta, Felipe A.; Ferrer, Mateus M.; Santana, Yuri V.B. de; Raubach, Cristiane W.; Longo, V. M.; Sambrano, Julio; Longo, Elson; Andres, Juan; Li, Maximo Siu; Varela, José A.
Metadatos
Mostrar el registro completo del ítemcomunitat-uji-handle:10234/9
comunitat-uji-handle2:10234/7013
comunitat-uji-handle3:10234/8638
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http://dx.doi.org/10.1016/j.jallcom.2012.12.081 |
Metadatos
Título
Synthesis of wurtzite ZnS nanoparticles using the microwave assisted solvothermal methodAutoría
Fecha de publicación
2013-04Editor
ElsevierISSN
0925-8388Cita bibliográfica
LA PORTA, Felipe A., et al. Synthesis of wurtzite ZnS nanoparticles using the microwave assisted solvothermal method. Journal of Alloys and Compounds, 2013, 556: 153-159.Tipo de documento
info:eu-repo/semantics/articleVersión de la editorial
http://www.sciencedirect.com/science/article/pii/S0925838812023055Versión
info:eu-repo/semantics/publishedVersionPalabras clave / Materias
Resumen
In this article, we report the development of an efficient and rapid microwave assisted solvothermal (MAS) method to prepare wurtzite ZnS nanoparticles at 413 K using different precursors. The materials obtained were ... [+]
In this article, we report the development of an efficient and rapid microwave assisted solvothermal (MAS) method to prepare wurtzite ZnS nanoparticles at 413 K using different precursors. The materials obtained were analyzed by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (MET) ultraviolet–visible (UV–vis) and photoluminescence (PL) measurements. The structure, surface chemical composition and optical properties were investigated as a function of the precursor. In addition, effects as well as merits of microwave heating on the processing and characteristics of ZnS nanoparticles obtained are reported. The possible formation mechanism and optical properties of these nanoparticles were also reported. [-]
Publicado en
Journal of Alloys and Compounds, 2013Derechos de acceso
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