Determination of albendazole and ivermectin residues in cattle and poultry-derived samples from India by micellar liquid chromatography
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Otros documentos de la autoría: Pawar, Rajendra-Prasad; Durgbanshi, Abhilasha; Bose, Devasish; Vives-Peris, Vicente; Albiol Chiva, Jaume; Esteve-Romero, Josep; Carda-Broch, Samuel
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https://doi.org/10.1016/j.jfca.2021.104111 |
Metadatos
Título
Determination of albendazole and ivermectin residues in cattle and poultry-derived samples from India by micellar liquid chromatographyAutoría
Fecha de publicación
2021-08-03Editor
ElsevierISSN
0889-1575Cita bibliográfica
PAWAR, Rajendra-Prasad, et al. Determination of albendazole and ivermectin residues in cattle and poultry-derived samples from India by micellar liquid chromatography. Journal of Food Composition and Analysis, 2021, vol. 103, p. 104111.Tipo de documento
info:eu-repo/semantics/articleVersión de la editorial
https://www.sciencedirect.com/journal/journal-of-food-composition-and-analysisVersión
info:eu-repo/semantics/publishedVersionPalabras clave / Materias
Resumen
We have developed a method, based on micellar liquid chromatography, to determine albendazole and ivermectin in dairy products and biological waste from bovine, as well as edible tissues from poultry. Anthelmitics ... [+]
We have developed a method, based on micellar liquid chromatography, to determine albendazole and ivermectin in dairy products and biological waste from bovine, as well as edible tissues from poultry. Anthelmitics were resolved in less than 10 min using a C18 column and a mobile phase of 0.15 mol/L sodium dodecyl sulfate – 6% 1-pentanol at buffered at pH 7 with a 0.01 M phosphate salt, running under isocratic mode at 1 mL/min. Detection was by absorbance at 292 nm. Method was successfully validated following official validation guidelines, in terms of: selectivity, sensitivity, calibration range (0.0125−0.5 mg/kg to 25−50 mg/kg), linearity (r2 > 9990), trueness (86.3–105.6%), precision (<12.2 %), carry-over effect, robustness and stability. Procedure was easy-to-conduct, safe, ecofriendly, economical and with a high sample throughput. It can be used as screening method prior to a confirmatory one, like liquid chromatography-mass spectrometry. Finally, it was applied to incurred samples. In nearly half of the food samples, the analytes were found at concentrations (albendazole 0.20–4.1 mg/kg and ivermectin, 0.31–8.73 mg/kg) over the maximum residue limits stated by international regulations. This exposes consumer to the risk of suffering from severe diseases and points out an inappropriate administration of anthelmitic-based treatments. [-]
Publicado en
Journal of Food Composition and Analysis Volume 103, October 2021, 104111Datos relacionados
https://ars.els-cdn.com/content/image/1-s2.0-S0889157521003112-mmc1.docxEntidad financiadora
Department of Science & Technology (Government of India) | Universitat Jaume I
Código del proyecto o subvención
Sl.No. 64 Dated 31−05-2016 | UJI-B2−018-20
Derechos de acceso
© 2021 Elsevier Inc. All rights reserved.
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