New insights on organosilane oligomerization mechanisms using ESI-MS and 29Si NMR
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Other documents of the author: Planelles Aragó, José; Vicent Barrera, Cristian; Julian-Lopez, Beatriz; Cordoncillo, Eloisa; Escribano López, Purificación
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comunitat-uji-handle2:10234/7053
comunitat-uji-handle3:10234/8639
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Title
New insights on organosilane oligomerization mechanisms using ESI-MS and 29Si NMRAuthor (s)
Date
2009Publisher
Royal Society of ChemistryISSN
1144-0546Bibliographic citation
PLANELLES ARAGÓ, Jose, et al. New insights on organosilane oligomerization mechanisms using ESI-MS and 29Si NMR. New Journal of Chemistry, 2009, vol. 33, no 5, p. 1100-1108.Type
info:eu-repo/semantics/articleSubject
Abstract
The use of electrospray ionization mass spectrometry (ESI-MS) in parallel with
29Si and 1H NMR to elucidate the aqueous speciation and temporal evolution of the
organosilane methyldiethoxysilane (MDES) through ... [+]
The use of electrospray ionization mass spectrometry (ESI-MS) in parallel with
29Si and 1H NMR to elucidate the aqueous speciation and temporal evolution of the
organosilane methyldiethoxysilane (MDES) through hydrolysis and condensation processes is
reported here. A suitable methodological approach for the monitoring of the oligomerization of
MDES under different pH conditions has been developed revealing details on the particular
oligomerization mechanism of this organosilane [-]
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New Journal of Chemistry, 2009, v. 33, n. 5Rights
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