Suzuki-Miyaura reaction catalized by palladium nanoparticles supported onto reduced graphene oxide
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Title
Suzuki-Miyaura reaction catalized by palladium nanoparticles supported onto reduced graphene oxideAuthor (s)
Tutor/Supervisor; University.Department
Mata Martínez, José Antonio; Universitat Jaume I. Departament de Química Inorgànica i OrgànicaDate
2019-07Publisher
Universitat Jaume IAbstract
The aim of this work is to study the catalytic properties of palladium nanoparticles
immobilized onto reduced graphene oxide. This objective can be divided into the following
items:
o Synthesis and characterization ... [+]
The aim of this work is to study the catalytic properties of palladium nanoparticles
immobilized onto reduced graphene oxide. This objective can be divided into the following
items:
o Synthesis and characterization of an imidazolium salt that would serve as ligand
precursor.
o Synthesis of a Pd-NHC complex and full characterization by 1H NMR, APT NMR,
1
H-1H COSY, 1H-13C HSQC, 1H-13C HMBC, MS, X-Ray diffraction and TGA.
o Immobilization and characterization by TEM and ICP-MS of the Pd-NHC complex
onto rGO.
o Formation of PdNPs immobilized onto rGO and full characterization by TEM, ICPMS and XPS.
o Study of the catalyst properties of the PdNPs immobilized onto rGO in the SuzukiMiyaura reaction.
o Study of recyclability of the PdNPs immobilized onto rGO in the Suzuki-Miyaura
reaction. [-]
Description
Treball Final de Grau en Química. Codi: QU0943. Curs acadèmic: 2018/2019
Type
info:eu-repo/semantics/bachelorThesisRights
http://rightsstatements.org/vocab/CNE/1.0/
info:eu-repo/semantics/restrictedAccess
info:eu-repo/semantics/restrictedAccess
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- Grau en Química [265]