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Determination of oxolinic acid, danofloxacin, ciprofloxacin, and enrofloxacin in porcine and bovine meat by micellar liquid chromatography with fluorescence detection
dc.contributor.author | Terrado Campos, David | |
dc.contributor.author | Tayeb Cherif, K. | |
dc.contributor.author | Vives-Peris, Vicente | |
dc.contributor.author | Carda-Broch, Samuel | |
dc.contributor.author | Esteve-Romero, Josep | |
dc.date.accessioned | 2017-08-31T07:27:39Z | |
dc.date.available | 2017-08-31T07:27:39Z | |
dc.date.issued | 2017-04-15 | |
dc.identifier.citation | TERRADO CAMPOS, David; TAYEB CHERIF, K.; PERIS VICENTE, Juan; CARDA BROCH, Samuel; ESTEVE ROMERO, Josep. Determination of oxolinic acid, danofloxacin, ciprofloxacin, and enrofloxacin in porcine and bovine meat by micellar liquid chromatography with fluorescence detection. Food Chemistry (2017), v. 221, p. 1277-1284 | ca_CA |
dc.identifier.uri | http://hdl.handle.net/10234/168529 | |
dc.description.abstract | A method was developed for the determination of oxolinic acid, danofloxacin, ciprofloxacin and enrofloxacin by micellar liquid chromatography – fluorescence detection in commercial porcine and bovine meat. The samples were ultrasonicated in a micellar solution, free of organic solvent, to extract the analytes, and the supernatant was directly injected. The quinolones were resolved in <22 min using a mobile phase of 0.05 M SDS – 7.5% 1-propanol – 0.5% triethylamine buffered at pH 3, running through a C18 column at 1 mL/min using isocratic mode. The method was validated by the in terms of: selectivity, calibration range (0.01–0.05 to 0.5 mg/kg), linearity (r2 > 0.9998), trueness (89.3–105.1%), precision (<8.3%), decision limit (<12% over the maximum residue limit), detection capability (<21% over the maximum residue limit), ruggedness (<5.6%) and stability. The procedure was rapid, eco-friendly, safe and easy-to-handle. | ca_CA |
dc.format.extent | 8 p. | ca_CA |
dc.format.mimetype | application/pdf | ca_CA |
dc.language.iso | eng | ca_CA |
dc.publisher | Elsevier | ca_CA |
dc.relation.isPartOf | Food Chemistry (2017), v. 221 | ca_CA |
dc.rights.uri | http://rightsstatements.org/vocab/CNE/1.0/ | * |
dc.subject | Flesh | ca_CA |
dc.subject | Food safety | ca_CA |
dc.subject | Micellar | ca_CA |
dc.subject | Quinolones | ca_CA |
dc.subject | Validation | ca_CA |
dc.title | Determination of oxolinic acid, danofloxacin, ciprofloxacin, and enrofloxacin in porcine and bovine meat by micellar liquid chromatography with fluorescence detection | ca_CA |
dc.type | info:eu-repo/semantics/article | ca_CA |
dc.identifier.doi | https://doi.org/10.1016/j.foodchem.2016.11.029 | |
dc.relation.projectID | This work was supported by Project P1.1B2012-36 del Pla de Promoció de la Investigació de la Universitat Jaume I (Spain). | ca_CA |
dc.rights.accessRights | info:eu-repo/semantics/restrictedAccess | ca_CA |
dc.relation.publisherVersion | http://www.sciencedirect.com/science/article/pii/S0308814616318520 | ca_CA |
dc.type.version | info:eu-repo/semantics/publishedVersion | ca_CA |
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