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3D printed flow reactors for the synthesis of single crystal perovskites
dc.contributor.author | Iglesias, Diego | |
dc.contributor.author | Tinajero Naranjo, Cristopher Alberto | |
dc.contributor.author | Luis Gómez, Jaume | |
dc.contributor.author | Aranda Alonso, Clara | |
dc.contributor.author | Martinez Cuenca, Raul | |
dc.contributor.author | Zanatta, Marcileia | |
dc.contributor.author | Sans, Victor | |
dc.date.accessioned | 2024-03-11T12:19:16Z | |
dc.date.available | 2024-03-11T12:19:16Z | |
dc.date.issued | 2024 | |
dc.identifier.citation | IGLESIAS, Diego, et al. 3D printed flow reactors for the synthesis of single crystal perovskites. Materials Today Energy, 2024, vol. 39, p. 101476. | ca_CA |
dc.identifier.uri | http://hdl.handle.net/10234/206129 | |
dc.description.abstract | Defect-free single crystal perovskites have unique photophysical properties that makes them highly attractive for a range of optoelectronic applications. However, their syntheses largely rely on batch protocols, which are limited in terms of reproducibility and scalability. Here, a new methodology is presented to develop tailored continuous-flow platforms for the synthesis of lead halide perovskites. The digital design of the reactors and their manufacturing with 3D printing, employing commercially available resins and low-cost stereolithography, was achieved. The reactor chamber was designed to facilitate the continuous slow addition of reagents to the reaction chamber, thus maintaining a constant concentration of reagents inside the reactor. The highly controlled synthetic conditions allowed for a high reproducibility of the crystallization process, with yields ranging between 8 and 15% in weight in eight consecutive reaction cycles. The crystals produced were characterized and demonstrated excellent photoluminescence properties. | ca_CA |
dc.format.extent | 9 p. | ca_CA |
dc.format.mimetype | application/pdf | ca_CA |
dc.language.iso | eng | ca_CA |
dc.publisher | Elsevier | ca_CA |
dc.relation.isPartOf | Materials Today Energy, 2024 | ca_CA |
dc.rights | 2468-6069/© 2023 The Author(s). Published by Elsevier Ltd. This is an open access article under the CC BY license | ca_CA |
dc.rights.uri | http://creativecommons.org/licenses/by/4.0/ | ca_CA |
dc.subject | Perovskites single crystal | ca_CA |
dc.subject | Crystallization | ca_CA |
dc.subject | Digitalization | ca_CA |
dc.subject | 3D printing | ca_CA |
dc.subject | Reactor design | ca_CA |
dc.title | 3D printed flow reactors for the synthesis of single crystal perovskites | ca_CA |
dc.type | info:eu-repo/semantics/article | ca_CA |
dc.identifier.doi | https://doi.org/10.1016/j.mtener.2023.101476 | |
dc.relation.projectID | info:eu-repo/grantAgreement/EC/H2020/101026335 | |
dc.rights.accessRights | info:eu-repo/semantics/openAccess | ca_CA |
dc.relation.publisherVersion | https://www.sciencedirect.com/science/article/pii/S2468606923002320 | ca_CA |
dc.type.version | info:eu-repo/semantics/publishedVersion | ca_CA |
project.funder.name | European Union's Horizon 2020 | ca_CA |
project.funder.name | Marie Skłodowska-Curie Individual Fellowships | ca_CA |
project.funder.name | Agencia Estatal de Investigación | ca_CA |
project.funder.name | Generalitat Valenciana | ca_CA |
project.funder.name | Universitat Jaume I | ca_CA |
project.funder.name | Ministerio de Universidades | ca_CA |
project.funder.name | Ministerio de Ciencia e Innovación | ca_CA |
project.funder.name | NextGeneration EU | ca_CA |
oaire.awardNumber | PID2020-119628RB-C33 | ca_CA |
oaire.awardNumber | MCIN/AEI/10.13039/501100011033 | ca_CA |
oaire.awardNumber | CIDEGENT 2018/036 | ca_CA |
oaire.awardNumber | CIGRIS/2021/075 | ca_CA |
oaire.awardNumber | FPU21/03740 | ca_CA |
oaire.awardNumber | TED2021-129758B-C33 | ca_CA |
oaire.awardNumber | MCIN/AEI/10.13039/501100011033/European Union NextGeneration EU/PRTR | ca_CA |
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