Unveiling the efficiency of microwave-assisted hydrothermal treatment for the preparation of SrTiO3 mesocrystals
![Thumbnail](/xmlui/bitstream/handle/10234/187321/68357.pdf.jpg?sequence=4&isAllowed=y)
Ver/ Abrir
Impacto
![Google Scholar](/xmlui/themes/Mirage2/images/uji/logo_google.png)
![Microsoft Academico](/xmlui/themes/Mirage2/images/uji/logo_microsoft.png)
Metadatos
Mostrar el registro completo del ítemcomunitat-uji-handle:10234/9
comunitat-uji-handle2:10234/7013
comunitat-uji-handle3:10234/8638
comunitat-uji-handle4:
INVESTIGACIONMetadatos
Título
Unveiling the efficiency of microwave-assisted hydrothermal treatment for the preparation of SrTiO3 mesocrystalsAutoría
Fecha de publicación
2019-09-16Editor
Royal Society of ChemistryISSN
1463-9076; 1463-9084Cita bibliográfica
: Phys. Chem. Chem. Phys., 2019, 21, 22031Tipo de documento
info:eu-repo/semantics/articleVersión de la editorial
https://pubs.rsc.org/en/content/articlelanding/2019/cp/c9cp02893e#!divAbstractVersión
info:eu-repo/semantics/acceptedVersionResumen
Material processing has become essential for the proper control, tuning and consequent application of
the properties of micro/nanoparticles. In this case, we report herein the capability of the microwaveassisted ... [+]
Material processing has become essential for the proper control, tuning and consequent application of
the properties of micro/nanoparticles. In this case, we report herein the capability of the microwaveassisted hydrothermal (MAH) method to prepare the SrTiO3 compound, as a case study of inorganic
compounds. Analyses conducted by X-ray diffraction, X-ray photoelectron and X-ray absorption
spectroscopies confirmed that the MAH route enables the formation of pristine SrTiO3. The results
indicated that the combination of thermal and non-thermal effects during the MAH treatment provides
ideal conditions for an efficient and rapid synthesis of pristine SrTiO3 mesocrystals. Scanning electron
microscopy images revealed a cube-like morphology (of ca. 1 mm) formed via a self-assembly process,
influenced by the MAH time. Additionally, photoluminescence measurements revealed a broad blue
emission related to intrinsic defects, which decreased with the MAH synthesis time. [-]
Publicado en
Physical Chemistry Chemical Physics, 2019, 21, 22031--22038Proyecto de investigación
XPS-22956, 88887.197794/2018-00 001, 442076/2014-2, 311463/2017-7, 405140/2018-5, 2013/07296-2, 2017/12437-5, UJIB2016-25, PrometeoII/2014/022, ACOMP/2014/270, ACOMP/2015/1202, CTQ2015-65207-P,, XAFS-20180311Derechos de acceso
This journal is © the Owner Societies 2019.
http://rightsstatements.org/vocab/InC/1.0/
info:eu-repo/semantics/openAccess
http://rightsstatements.org/vocab/InC/1.0/
info:eu-repo/semantics/openAccess
Aparece en las colecciones
- QFA_Articles [825]