Procedure for the Screening of Eggs and Egg Products to Detect Oxolonic Acid, Ciprofloxacin, Enrofloxacin, and Sarafloxacin Using Micellar Liquid Chromatography
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Other documents of the author: Vives-Peris, Vicente; García Ferrer, Daniel; Mishra, Pooja; Albiol Chiva, Jaume; Durgbanshi, Abhilasha; Carda-Broch, Samuel; Bose, Devasish; Esteve-Romero, Josep
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Title
Procedure for the Screening of Eggs and Egg Products to Detect Oxolonic Acid, Ciprofloxacin, Enrofloxacin, and Sarafloxacin Using Micellar Liquid ChromatographyAuthor (s)
Date
2019-11-15Publisher
MDPIISSN
2079-6382Bibliographic citation
Peris-Vicente, J.; García-Ferrer, D.; Mishra, P.; Albiol-Chiva, J.; Durgbanshi, A.; Carda-Broch, S.; Bose, D.; Esteve-Romero, J. Procedure for the Screening of Eggs and Egg Products to Detect Oxolonic Acid, Ciprofloxacin, Enrofloxacin, and Sarafloxacin Using Micellar Liquid Chromatography. Antibiotics 2019, 8, 226Type
info:eu-repo/semantics/articlePublisher version
https://www.mdpi.com/2079-6382/8/4/226/htmVersion
info:eu-repo/semantics/publishedVersionSubject
Abstract
A method based on micellar liquid chromatography was developed to determine oxolinic acid, ciprofloxacin, enrofloxacin, and sarafloxacin in eggs and egg products. The antimicrobial drugs were obtained in a micellar ... [+]
A method based on micellar liquid chromatography was developed to determine oxolinic acid, ciprofloxacin, enrofloxacin, and sarafloxacin in eggs and egg products. The antimicrobial drugs were obtained in a micellar solution which was directly injected. The analytes were resolved using a C18 column and a mobile phase of 0.05 M sodium dodecyl sulfate—7.5% 1-propanol—0.5% triethylamine, buffered at pH 3 with phosphate salt, running under the isocratic mode. The signal was monitored by fluorescence. Validation was successfully performed according to the EU Commission Decision 2002/657/EC in terms of specificity, calibration range (LOQ to 1 mg/kg), linearity (R2 > 0.9991), limit of detection and decision limit (0.01–0.05 mg/kg), limit of quantification (0.025–0.150 mg/kg), detection capability (<0.4 times decision limit), trueness (−14.2% to +9.8%), precision (<14.0%), robustness, and stability. The procedure was environmentally friendly, safe, easy-to-conduct, inexpensive, and had a high sample throughput, thus it is useful for routine analysis as a screening method in a laboratory for food residue control. [-]
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Antibiotics, 2019, vol. 8, no 4Investigation project
Regional Valencian Government “Generalitat Valenciana” research project number: AICO/2017/063; University Jaume I research project number: UJI-B2018-20Rights
info:eu-repo/semantics/openAccess
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