Gas chromatographic analysis of fatty acid methyl esters of milk fat by an ionic liquid derived from L-phenylalanine as the stationary phase
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Other documents of the author: González, Laura; González Álvarez, Jaime; Fernández Gonzalo, Carla; Arias Abrodo, Pilar; Altava, Belen; Luis, Santiago V.; Burguete, M. Isabel; Gutiérrez Álvarez, María Dolores
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http://dx.doi.org/10.1016/j.talanta.2015.05.036 |
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Title
Gas chromatographic analysis of fatty acid methyl esters of milk fat by an ionic liquid derived from L-phenylalanine as the stationary phaseAuthor (s)
Date
2015-10Publisher
ElsevierBibliographic citation
Mendoza, Laura González, et al. "Gas chromatographic analysis of fatty acid methyl esters of milk fat by an ionic liquid derived from L-phenylalanine as the stationary phase." Talanta 143 (2015): 212-218.Type
info:eu-repo/semantics/articlePublisher version
http://www.sciencedirect.com/science/article/pii/S0039914015004002Subject
Abstract
A Gas Chromatography (GC) method has been developed for the separation and characterization of the different fatty acids in anhydrous milk fat (AMF) by means of an ionic liquid stationary phase, characterized by a ... [+]
A Gas Chromatography (GC) method has been developed for the separation and characterization of the different fatty acids in anhydrous milk fat (AMF) by means of an ionic liquid stationary phase, characterized by a monocationic imidazolium salt derived from l-phenylalanine. The inner surface of a fused silica capillary column was modified using this ionic liquid functionality and 3-aminopropyldiethoxymethyl silane. This coated GC column, which exhibited good thermal stability (270 °C) and good efficiency (2700 plates/m), has been characterized using the Abraham solvation parameter model. The intra-day and inter-day precision of the method have been evaluated, obtaining relative standard deviations (RSD) from 0.99% to 4.0% and from 2.8% to 9.2%, respectively. Furthermore, recoveries from 90% and 99% have been achieved. [-]
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Talanta Volume 143, 1 October 2015Rights
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