Organometallic derivatives of Rh- and Ir-substituted polyoxotungstates with Keggin structure: reactivity screening by electrospray ionization mass-spectrometry
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Altres documents de l'autoria: Sokolov, Maxim; Adonin, Sergey A.; Sinkevich, Pavel L.; Vicent Barrera, Cristian; Mainichev, Dmitry A.; Fedin, Vladimir P.
Metadades
Mostra el registre complet de l'elementcomunitat-uji-handle:10234/9
comunitat-uji-handle2:10234/7013
comunitat-uji-handle3:10234/8638
comunitat-uji-handle4:
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http://dx.doi.org/10.1039/C2DT30655G |
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Títol
Organometallic derivatives of Rh- and Ir-substituted polyoxotungstates with Keggin structure: reactivity screening by electrospray ionization mass-spectrometryAutoria
Data de publicació
2012-06Editor
Royal Society of ChemistryTipus de document
info:eu-repo/semantics/articleVersió de l'editorial
http://pubs.rsc.org/en/content/articlepdf/2012/dt/c2dt30655gVersió
info:eu-repo/semantics/publishedVersionResum
ESI-MS based methodology for the rapid reactivity screening of [PW11O39RhCl]5− and [PW11O39Ir(H2O)]4− toward various metalation-intended substrates (reagents with an activated C–H bond, boronic acids and organotin ... [+]
ESI-MS based methodology for the rapid reactivity screening of [PW11O39RhCl]5− and [PW11O39Ir(H2O)]4− toward various metalation-intended substrates (reagents with an activated C–H bond, boronic acids and organotin compounds) is presented. Formation of a series of new organometallic POM derivatives with Rh–R (R = malonate, phenylacetate, CH3, Ph, ferrocenyl) and Ir–R (R = CH3) bonds is reported. [-]
Publicat a
Dalton Transactions. 2012, 41Drets d'accés
© The Royal Society of Chemistry 2012
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