Detection of most commonly used pesticides in green leafy vegetables from sagar, india using direct injection hybrid micellar liquid chromatography
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Otros documentos de la autoría: Bhamdare, Hemlata; Pahade, Priyanka; Bose, Devasish; Durgbanshi, Abhilasha; Carda-Broch, Samuel; Peris Vicente, Juan
Metadatos
Mostrar el registro completo del ítemcomunitat-uji-handle:10234/9
comunitat-uji-handle2:10234/7013
comunitat-uji-handle3:10234/8638
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INVESTIGACIONMetadatos
Título
Detection of most commonly used pesticides in green leafy vegetables from sagar, india using direct injection hybrid micellar liquid chromatographyAutoría
Fecha de publicación
2022-05Editor
ElsevierISSN
2772-5820Cita bibliográfica
Bhamdare, H., Pahade, P., Bose, D., Durgbanshi, A., Carda-Broch, S., & Peris-Vicente, J. (2022). Detection of most commonly used pesticides in green leafy vegetables from Sagar, India using direct injection hybrid micellar liquid chromatography. Advances in Sample Preparation, 2, 100015Tipo de documento
info:eu-repo/semantics/articleVersión de la editorial
https://www.sciencedirect.com/science/article/pii/S2772582022000122Versión
info:eu-repo/semantics/publishedVersionPalabras clave / Materias
Resumen
Imidacloprid, chlorpyrifos, profenofos and cypermethrin are most commonly applied pesticides on green leafy vegetables. After a survey conducted to know the pesticide management practices in Sagar, India, a procedure ... [+]
Imidacloprid, chlorpyrifos, profenofos and cypermethrin are most commonly applied pesticides on green leafy vegetables. After a survey conducted to know the pesticide management practices in Sagar, India, a procedure based on hybrid micellar liquid chromatography coupled to a photodiode array detector has been developed and validated to monitor imidacloprid, chlorpyrifos, profenofos and cypermethrin content in green leafy vegetables. The method was validated following the guideline of SANTE/11,312/2021 in terms of: selectivity, linearity (r2> 0.998), limit of quantification (0.09–0.25 mg/Kg, depending on the analyte under investigation), precision (<8.1%), and robustness (<5%). Chlorpyrifos was found to be the most commonly used pesticide among vegetable growers. It was found in seventy-six percent samples, profenofos in fifty-one percent, imidacloprid in eight percent and cypermethrin in four percent of the analyzed green leafy vegetable sample either individually or in combination. Sixteen percent of the collected samples were found to be negative for the selected pesticides. The developed procedure is rapid, easy to handle, green since it uses a low amount of toxic chemicals providing reliable results. The method was used to evaluate the eventual correlation between the analytical data and the information collected from the producers and users of these pesticides. [-]
Publicado en
Advances in Sample Preparation, 2022, vol. 2Entidad financiadora
Ministerio de Ciencia, Innovación y Universidades | University Grant Commission (UGC)
Identificador de la entidad financiadora
http://dx.doi.org/10.13039/501100011033
Código del proyecto o subvención
MICIU/ICTI2017-2020/PID2019-106708GB-I00 | UGC-Ref.No.3354/(OBC)(NET-DEC.2015) | UGC-Ref.No.3335/(Sc) (NET-DEC.2015)
Título del proyecto o subvención
Estudios fundamentales y diseño de estrategias en cromatografía líquida mono- y bi-dimensional para potenciar la calidad de las separaciones de muestras complejas
Derechos de acceso
info:eu-repo/semantics/openAccess
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