A general method to determine optimal thermal cycles based on solid-state sintering fundamentals
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Título
A general method to determine optimal thermal cycles based on solid-state sintering fundamentalsFecha de publicación
2019-04-01Editor
ElsevierISSN
0272-8842; 1873-3956Cita bibliográfica
BARBA-JUAN, Antonio; CLAUSELL-TEROL, Carolina. A general method to determine optimal thermal cycles based on solid-state sintering fundamentals. Ceramics International, 2019, vol. 45, no 5, p. 5346-5354Tipo de documento
info:eu-repo/semantics/articleVersión de la editorial
https://www.sciencedirect.com/science/article/pii/S0272884218333534Versión
info:eu-repo/semantics/submittedVersionPalabras clave / Materias
Resumen
Most technical ceramics require processing up to and including final-stage sintering to obtain a high-density bulk while inhibiting grain growth as dominant sintering process as far as possible. The literature typically ... [+]
Most technical ceramics require processing up to and including final-stage sintering to obtain a high-density bulk while inhibiting grain growth as dominant sintering process as far as possible. The literature typically highlights the qualitative interdependence of the sintering variables and microstructural parameters, focusing on very simple particulate systems. However, a quantitative method to achieve optimum sintering of actual polycrystalline solids is still lacking.
This paper puts forward such a method, which has been satisfactorily tested by the authors. The method consists of a mathematical model, based on the physical phenomena that take place during solid-state sintering. The method leads to two differential equations: a densification rate and a pore-dragged normal grain growth rate equation during final-stage sintering, which mainly depend on sintering temperature and shaping conditions. Simultaneous numerical integration of these two rate equations allows design of an optimal thermal cycle (enhancing densification and controlling grain growth) to obtain the targeted sintered polycrystalline microstructure. Application of this method yields staggered thermal cycles, in addition to the number of steps, as well as the sintering temperature and dwell time in each step. [-]
Publicado en
Ceramics International, 2019, vol. 45, no 5Proyecto de investigación
Spanish National Plan for Scientific Research, Development, and Technology Innovation of the Spanish Ministry of Economy and Competitiveness: MAT2016-76320-R; Jaume I University of Spain: UJI-B2017-48Derechos de acceso
Copyright © Elsevier B.V.
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