A rapid and reliable assay to determine flumequine, marbofloxacin, difloxacin, and sarafloxacin in commonly consumed meat by micellar liquid chromatography
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Otros documentos de la autoría: Vives-Peris, Vicente; Iborra‐Millet, Jesús Javier; Albiol Chiva, Jaume; Carda-Broch, Samuel; Esteve-Romero, Josep
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https://doi.org/10.1002/jsfa.9314 |
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Título
A rapid and reliable assay to determine flumequine, marbofloxacin, difloxacin, and sarafloxacin in commonly consumed meat by micellar liquid chromatographyAutoría
Fecha de publicación
2018-10Editor
WileyCita bibliográfica
PERIS‐VICENTE, Juan, et al. A rapid and reliable assay to determine flumequine, marbofloxacin, difloxacin, and sarafloxacin in commonly consumed meat by micellar liquid chromatography. Journal of the Science of Food and Agriculture, 2019; 99 : 1375–1383.Tipo de documento
info:eu-repo/semantics/articleVersión de la editorial
https://onlinelibrary.wiley.com/doi/full/10.1002/jsfa.9314Versión
info:eu-repo/semantics/publishedVersionPalabras clave / Materias
Resumen
BACKGROUND: Micellar liquid chromatography – fluorescence detection was used to determine the antibiotics flumequine,
marbofloxacin, difloxacin, and sarafloxacin in porcine, bovine, poultry, ovine, caprine, rabbit, ... [+]
BACKGROUND: Micellar liquid chromatography – fluorescence detection was used to determine the antibiotics flumequine,
marbofloxacin, difloxacin, and sarafloxacin in porcine, bovine, poultry, ovine, caprine, rabbit, and equine meat, to verify
compliance with EU Regulation 37/2010 with regard to the occurrence of veterinary drugs in food.
RESULTS: The analytes were isolated from the matrix by ultrasonication-assisted leaching in a micellar solution, and the
supernatant was filtered and directly injected. The fluoroquinolones were resolved in
<
19 min using a C18 column, with an
isocratic mobile phase of 0.05 mol L
−
1
sodium dodecyl sulfate - 8% 1-butanol – 0.5% triethylamine buffered at pH 3. The limits
of quantification (0.01–0.05 mg kg
−
1
) were below the maximum residue limits (0.15–0.4 mg kg
−
1
). The method was validated
by EU Commission Decision 2002/657/EC guidelines.
CONCLUSION: The method shows practical advantages such as simplicity, low cost, eco-friendliness, safety, and applicability for
routine analysis, and is useful for surveillance programs. [-]
Proyecto de investigación
Generalitat Valenciana (Grant Number: AICO/2017/063)Derechos de acceso
© 2018 Society of Chemical Industry
http://rightsstatements.org/vocab/InC/1.0/
info:eu-repo/semantics/restrictedAccess
http://rightsstatements.org/vocab/InC/1.0/
info:eu-repo/semantics/restrictedAccess
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