Determination of oxolinic acid, danofloxacin, ciprofloxacin, and enrofloxacin in porcine and bovine meat by micellar liquid chromatography with fluorescence detection
Impacte
Scholar |
Altres documents de l'autoria: Terrado Campos, David; Tayeb Cherif, K.; Vives-Peris, Vicente; Carda-Broch, Samuel; Esteve-Romero, Josep
Metadades
Mostra el registre complet de l'elementcomunitat-uji-handle:10234/9
comunitat-uji-handle2:10234/7013
comunitat-uji-handle3:10234/8638
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INVESTIGACIONAquest recurs és restringit
https://doi.org/10.1016/j.foodchem.2016.11.029 |
Metadades
Títol
Determination of oxolinic acid, danofloxacin, ciprofloxacin, and enrofloxacin in porcine and bovine meat by micellar liquid chromatography with fluorescence detectionAutoria
Data de publicació
2017-04-15Editor
ElsevierCita bibliogràfica
TERRADO CAMPOS, David; TAYEB CHERIF, K.; PERIS VICENTE, Juan; CARDA BROCH, Samuel; ESTEVE ROMERO, Josep. Determination of oxolinic acid, danofloxacin, ciprofloxacin, and enrofloxacin in porcine and bovine meat by micellar liquid chromatography with fluorescence detection. Food Chemistry (2017), v. 221, p. 1277-1284Tipus de document
info:eu-repo/semantics/articleVersió de l'editorial
http://www.sciencedirect.com/science/article/pii/S0308814616318520Versió
info:eu-repo/semantics/publishedVersionParaules clau / Matèries
Resum
A method was developed for the determination of oxolinic acid, danofloxacin, ciprofloxacin and enrofloxacin by micellar liquid chromatography – fluorescence detection in commercial porcine and bovine meat. The samples ... [+]
A method was developed for the determination of oxolinic acid, danofloxacin, ciprofloxacin and enrofloxacin by micellar liquid chromatography – fluorescence detection in commercial porcine and bovine meat. The samples were ultrasonicated in a micellar solution, free of organic solvent, to extract the analytes, and the supernatant was directly injected. The quinolones were resolved in <22 min using a mobile phase of 0.05 M SDS – 7.5% 1-propanol – 0.5% triethylamine buffered at pH 3, running through a C18 column at 1 mL/min using isocratic mode. The method was validated by the in terms of: selectivity, calibration range (0.01–0.05 to 0.5 mg/kg), linearity (r2 > 0.9998), trueness (89.3–105.1%), precision (<8.3%), decision limit (<12% over the maximum residue limit), detection capability (<21% over the maximum residue limit), ruggedness (<5.6%) and stability. The procedure was rapid, eco-friendly, safe and easy-to-handle. [-]
Publicat a
Food Chemistry (2017), v. 221Proyecto de investigación
This work was supported by Project P1.1B2012-36 del Pla de Promoció de la Investigació de la Universitat Jaume I (Spain).Drets d'accés
http://rightsstatements.org/vocab/CNE/1.0/
info:eu-repo/semantics/restrictedAccess
info:eu-repo/semantics/restrictedAccess
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