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dc.contributor.authorCherta Cucala, Laura
dc.contributor.authorBeltrán Arandes, Joaquim
dc.contributor.authorLópez, Francisco
dc.contributor.authorHernández Hernández, Félix
dc.date.accessioned2014-03-10T17:56:11Z
dc.date.available2014-03-10T17:56:11Z
dc.date.issued2013
dc.identifier.citationFood Analytical Methods August 2013, Volume 6, Issue 4, pp 1170-1187ca_CA
dc.identifier.issn1936-9751
dc.identifier.issn1936-976X
dc.identifier.urihttp://hdl.handle.net/10234/86429
dc.description.abstractA fast gas chromatography–mass spectrometry method has been developed for multiresidue determination of up to 56 pesticides in fruits and vegetables in a chromatographic run time of <10 min, using a single quadrupole mass spectrometer operating in selected ion monitoring mode. The well-known acetate-buffering version of the QuEChERS method has been used for sample preparation. Programmable temperature vaporizer injection of 3 μL allowed reaching limits of detection between 0.15 and 15 μg/kg for most compounds in the sample matrices tested. The applicability of the method has been evaluated in apple, orange, carrot, and tomato. Recoveries at three fortification levels (0.01, 0.1 and 0.5 mg/kg) ranged from 70 to 120 % for most compounds, with relative standard deviations below 20 % in all cases. The developed method has been applied to fruit and vegetable samples from different Spanish provinces.ca_CA
dc.format.extent34 p.ca_CA
dc.format.mimetypeapplication/pdfca_CA
dc.language.isoengca_CA
dc.publisherSpringer Verlagca_CA
dc.relation.isPartOfFood Analytical Methods August, 2013, Vol. 6, No 4ca_CA
dc.rights© Springer Science+Business Media New York 2012. The final publication is available at Springer via http://dx.doi.org/10.1007/s12161-012-9524-1ca_CA
dc.subjectPesticidesca_CA
dc.subjectFast gas chromatography–mass spectrometryca_CA
dc.subjectFruits and vegetablesca_CA
dc.subjectMatrix effectsca_CA
dc.subjectQuEChERSca_CA
dc.titleApplication of Fast Gas Chromatography–Mass Spectrometry in Combination with the QuEChERS Method for the Determination of Pesticide Residues in Fruits and Vegetablesca_CA
dc.typeinfo:eu-repo/semantics/articleca_CA
dc.identifier.doihttp://dx.doi.org/10.1007/s12161-012-9524-1
dc.rights.accessRightsinfo:eu-repo/semantics/openAccessca_CA
dc.relation.publisherVersionhttp://link.springer.com/article/10.1007%2Fs12161-012-9524-1ca_CA


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